**章化学实验室基础知识1 第二章实验部分16 实验一溶胶-凝胶法制备纳米二氧化钛16 Experiment 1Preparation of Nano-TiO2 by Sol-Gel Method17 实验二XRD分析纳米二氧化钛的晶相20 Experiment 2Phase characterization of Nano-TiO2 powder by XRD22 实验三纳米二氧化钛光催化降解染料25 Experiment 3Photocatalytic degradation of dyes by Nano-TiO227 实验四乙酰二茂铁的制备29 Experiment 4Preparation of Acetylferrocene32 实验五乙酰二茂铁粗产物的重结晶及红外光谱测定36 Experiment 5Recrystallization of crude products of acetylferrocene and its characterization by infrared spectroscopy38 实验六乙酰二茂铁的熔点和1H NMR测定41 Experiment 6Determination of melting point and 1H NMR of ferrocene43 实验七聚苯胺的电化学合成46 Experiment 7Electrosynthesis of Polyaniline48 实验八聚苯胺导电聚合物膜的pH响应50 Experiment 8pH response of polyaniline conductive polymer film51 实验九2-氨基-1,3,4-噻二唑的制备53 Experiment 9Synthesis of 2-amino-1,3,4-thiadiazole54 实验十反相离子对色谱法分析2-氨基-1,3,4噻二唑的含量56 Experiment 10Ion pair reversed phaser chromatographic separation and quantitation of 2-amino-1,3,4-thiadiazole59 实验十一聚丙烯酸合成63 Experiment 11Synthesis of Polyacrylic acid65 实验十二黏度法测定水溶性高聚物的平均分子量68 Experiment 12Determination of the average relative molecular weight of water-soluble polymer by viscosity method73 实验十三酶催化分光光度法测定过氧化氢80 Experiment 13Determination of hydrogen peroxide by enzyme catalytic spectrophotometry82 实验十四磷酸的电位滴定84 Experiment 14Potentiometric titration of phosphoric acid86 实验十五对乙酰氨基酚的电化学反应机理及其浓度的测定89 Experiment 15Study on the electrochemical reaction mechanism of acetaminophen and determination of its concentration91 实验十六ZnS:Mn纳米荧光材料的合成及其光学性质研究95 Experiment 16Synthesis and optical properties of ZnS:Mn fluorescent nanomaterials97 实验十七8-羟基喹啉铝的合成和荧光性能表征99 Experiment 17Synthesis and fluorescence characterization of 8-hydroxyquinoline aluminum102 实验十八有机螺环染料的荧光特性及其定量分析106 Experiment 18Fluorescence characteristics and quantitative analysis of organic spiro dyes110 实验十九离子液体bmimBF4的制备114 Experiment 19Synthesis of the ionic liquid bmimBF4116 实验二十柠檬精油的提取117 Experiment 20Extraction of lemon essential oil119 实验二十一柠檬精油的GC-MS分析120 Experiment 21GC-MS analysis of lemon essential oil122 实验二十二钛硅分子筛的合成123 Experiment 22Synthesis of titanium silicalite molecular sieve(TS-1)126 实验二十三钛硅分子筛的表征(SEM)129 Experiment 23Characterization of titanium silicalite molecular sieve TS-1(SEM)131 实验二十四钛硅分子筛催化苯酚制备苯二酚134 Experiment 24Preparation of hydroquinone from phenol catalyzed by titanium silicalite molecular sieve137 附录141 附录一X射线衍射仪操作规程141 附录二SEM使用操作流程142 附录三Agilent 7890B/5977A气质联用仪操作规程143 附录四**液相色谱仪器操作规程146 附录五电极的使用说明150 附录六奥立龙CHN060型酸度计的操作规程151 附录七显微熔点仪操作规程151 附录八CHI 660电化学工作站操作规程152 附录九Bruker 400MHz核磁共振谱仪操作规程153 附录十FluoroMax-4荧光光谱仪操作规程156 参考文献159