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Contents Preface Chapter 1 Environmental Operation and Expression 1 1.1 Environmental Operation and Process 1 1.2 Treatment of Monitoring Results 2 1.3 Expression of Monitoring Results 2 1.4 Monitoring Errors and Treatment 5 1.5 Atmospheric Environment and Pollutants 15 1.6 Atmospheric Pollutants Concentration 17 1.7 Detection Limit， Precision and Accuracy in Atmospheric Monitoring Analysis 18 1.8 Reference Material and Quality Control 23 Chapter 2 Sampling Method of Atmospheric Environment Samples 28 2.1 Sampling Principle 28 2.2 Sampling Devices and Systems 33 2.3 Quality Control and Quality Assurance 35 Chapter 3 Preparation of Atmospheric Environment Samples 37 3.1 Sample Pretreatment 37 3.2 Sample Storage 39 3.3 Pre-preparation of Sample Analysis 39 3.4 Sample Decomposition 41 Chapter 4 Standard Gas and Its Preparation Method 44 4.1 Concept of Standard Gas 44 4.2 Preparation Principle and Method 44 Chapter 5 Monitoring of Atmospheric Environmental Solid Contaminants 48 Monitoring 1 Atmospheric Dust Sampling and Monitoring 48 Monitoring 2 Concentration Monitoring of TSP in Atmospheric Environment 53 Monitoring 3 Monitoring of Inhalable Particles (IP) in Atmospheric Environment 56 Monitoring 4 Monitoring of Dust Concentration in Atmosphere of Flue Gas Pollution 59 Chapter 6 Monitoring of Atmospheric Environmental Inorganic Gaseous Pollutants 63 Monitoring 5 Monitoring of CO2 in Atmosphere by Aus-gas Analyzer 63 Monitoring 6 Monitoring of CO Concentration in Atmospheric Environment 68 Monitoring 7 Monitoring of SO2 Concentration in Atmospheric Environment 71 Monitoring 8 Monitoring of NOX Concentration in Atmospheric Environment 76 Monitoring 9 Joint Monitoring of SO2 and NOX Concentration in Atmospheric Environment 81 Monitoring 10 Monitoring of NH3 Concentration in Atmospheric Environment 84 Monitoring 11 Monitoring of HCN Concentration in Atmospheric Environment 88 Monitoring 12 Monitoring of Fluoride Concentration in Atmospheric Environment 93 Monitoring 13 Monitoring of O3 Concentration in Atmospheric Environment 97 Monitoring 14 Monitoring of H2S Concentration in Atmospheric Environment 101 Monitoring 15 Monitoring of HCl Concentration in Atmospheric Environment 105 Monitoring 16 Monitoring of Cl2 Concentration in Atmospheric Environment 108 Monitoring 17 Monitoring of Hg Concentration in Atmospheric Environment 111 Monitoring 18 Monitoring of Pb Concentration in Atmospheric Environment 115 Monitoring 19 Monitoring of Polycyclic Aromatic Hydrocarbons Concentration in Atmospheric Environment 118 Monitoring 20 Monitoring of Polychlorinated Dibenzo-p-dioxins Concentration in Atmospheric Environment 125 Chapter 7 Monitoring of Atmospheric Organic Pollutants 133 Monitoring 21 Monitoring of Polychlorinated Biphenyls in Atmospheric Environment 133 Monitoring 22 Monitoring of Aromatic Hydrocarbon Pollutants in Atmospheric Environment 140 Monitoring 23 Monitoring of Hormone Pollutants in Atmospheric Environment 143 Monitoring 24 Monitoring of Organic Pesticide Pollutants in Atmospheric Environment 146 Monitoring 25 Monitoring of Aldehyde Pollutants in Atmospheric Environment 149 Monitoring 26 Monitoring of Ketone Pollutants in Atmospheric Environment 153 Monitoring 27 Monitoring of Phenolic Pollutants in Atmospheric Environment 155 Monitoring 28 Monitoring of Alcohol Pollutants in Atmospheric Environment 160 Monitoring 29 Monitoring of Phosgene Pollutants in Atmospheric Environment 164 Monitoring 30 Monitoring of Amine Pollutants in Atmospheric Environment 167 Monitoring 31 Monitoring of Hydrazine Pollutants in Atmospheric Environment 173 Monitoring 32 Monitoring of Nitrile Pollutants in Atmospheric Environment 177 Monitoring 33 Monitoring of Odor Gas Pollutants in Atmospheric Environment 182 Monitoring 34 Monitoring of Total Alkane Pollutants in Atmospheric Environment 184 Chapter 8 Monitoring of Other Pollutants in Air 189 Monitoring 35 Monitoring of Indoor Air Pollutants 189 Monitoring 36 Monitoring of Vehicle Exhaust Pollution 192 Monitoring 37 Monitoring of Smoke and Exhaust Pollutants in Restaurants 198 References 202 Appendix 203 Appendix 1 Standard Total Ion Chromatogram of PAHs 203 Appendix 2 Liquid Chromatographic Reference Plots of Standards of Thirteen Aldehydes， Ketones and Hydrazone 203 Appendix 3 Standard Liquid Chromatogram of Phenolic Compounds 204